Meyer, Tjark Hannes

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[["dc.bibliographiccitation.firstpage","2890"],["dc.bibliographiccitation.issue","8"],["dc.bibliographiccitation.journal","Chemical Science"],["dc.bibliographiccitation.lastpage","2897"],["dc.bibliographiccitation.volume","12"],["dc.contributor.author","Meyer, Tjark H."],["dc.contributor.author","Samanta, Ramesh C."],["dc.contributor.author","Del Vecchio, Antonio"],["dc.contributor.author","Ackermann, Lutz"],["dc.date.accessioned","2021-06-01T09:41:45Z"],["dc.date.available","2021-06-01T09:41:45Z"],["dc.date.issued","2021"],["dc.description.abstract","The merger of manganese-catalyzed C–H functionalization with electrosynthesis enabled C(sp 3 )–H azidation devoid of chemical oxidants or photochemical irradiation. Detailed mechanistic studies are supportive of a manganese( iii/iv ) electrocatalysis."],["dc.description.abstract","Manganaelectro-catalyzed azidation of otherwise inert C(sp 3 )–H bonds was accomplished using most user-friendly sodium azide as the nitrogen-source. The operationally simple, resource-economic C–H azidation strategy was characterized by mild reaction conditions, no directing group, traceless electrons as the sole redox-reagent, Earth-abundant manganese as the catalyst, high functional-group compatibility and high chemoselectivity, setting the stage for late-stage azidation of bioactive compounds. Detailed mechanistic studies by experiment, spectrophotometry and cyclic voltammetry provided strong support for metal-catalyzed aliphatic radical formation, along with subsequent azidyl radical transfer within a manganese( iii / iv ) manifold."],["dc.identifier.doi","10.1039/D0SC05924B"],["dc.identifier.uri","https://resolver.sub.uni-goettingen.de/purl?gro-2/85028"],["dc.language.iso","en"],["dc.notes.intern","DOI-Import GROB-425"],["dc.relation.eissn","2041-6539"],["dc.relation.issn","2041-6520"],["dc.title","Mangana( iii / iv )electro-catalyzed C(sp 3 )–H azidation"],["dc.type","journal_article"],["dc.type.internalPublication","yes"],["dspace.entity.type","Publication"]]